Journal
INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
Volume 49, Issue 22, Pages 11310-11320Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ie101346u
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Funding
- US National Science Foundation [CHE-0714189]
- US Army Research Office through the Institute for Soldier Nanotechnology [DAAD-19-02-0002]
- GIS
- MIT-France
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The development of chemically compatible microsystems that can operate across expanded process conditions, such as high pressures (HP) and high temperatures (HT), is of great interest for many applications, including high pressure chemistry and hydrothermal and supercritical fluid processes. We present a methodology for the successful design and use of HP/HT microsystems. Key parameters for the fabrication of microreactors and modular fluidic packaging able to withstand severe pressure and temperature conditions (30 MPa, 400 degrees C) are described. Applications of these HP/HT plug and play microsystems are illustrated with examples, including multiphase flow visualization through the transition of liquid-liquid immiscible hexane-water segmented flow to homogeneous supercritical flow, on chip supercritical water oxidation, and synthesis of iron oxide nanoparticles.
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