Journal
MATERIALS RESEARCH-IBERO-AMERICAN JOURNAL OF MATERIALS
Volume 18, Issue 5, Pages 953-956Publisher
UNIV FED SAO CARLOS, DEPT ENGENHARIA MATERIALS
DOI: 10.1590/1516-1439.359114
Keywords
mechanical alloying; semiconductors; electrical properties
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Funding
- CNPq [448041/2014-6, 300821/2012-3]
- FAPEMIG
- FUNEPU
- FAPESP [2009/54001-2]
- Fundacao de Amparo a Pesquisa do Estado de Sao Paulo (FAPESP) [09/54001-2] Funding Source: FAPESP
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In this work we demonstrate that high-energy ball milling process can be used to synthesize SnSb2Te4 without surfactant and further annealing. Milling parameters such as ball to raw material ratio (5:1) and milling time (2h) were determined to be suitable for synthesizing microplatelets of SnSb2Te4. The powders after milling for various durations were characterized by X-ray powder diffraction, scanning electron microscopy and electrical resistance measurements.
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