4.6 Article

To promote the nucleation and growth of graphene in arc discharge process by magnetic field and H2

Journal

MATERIALS LETTERS
Volume 159, Issue -, Pages 43-46

Publisher

ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2015.05.177

Keywords

Carbon materials; Arc discharge; Scanning electron microscopy; Raman

Funding

  1. Xinjiang Autonomous Region Major Projects [201130113-1]
  2. National Natural Science Foundation of China [U1203292]
  3. Technological Innovation Youth Training Project of Xinjiang Autonomous [2013731006]
  4. Science and Technology Assistance of Xinjiang Province [201491126]
  5. Western Light Talent Culture Project of Chinese Academy of Sciences [YBXM-2014-07]

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Few-layer graphene sheets were synthesized by magnetic field induced arc discharge method using He-H-2 mixture as buffer gas and Ni-Y2O3 powder as catalyst The effect of hydrogen pressure, magnetic field, and Ni-Y2O3 catalyst were studied with respect to the morphology and structure of the synthesized carbon materials. The samples were characterized by SEM, TEM, TGA and Raman spectroscopy. The SEM images and Raman spectroscopy results revealed that the hydrogen pressure and magnetic field played a key role in the catalytic growth of graphene. High resolution TEM analysis showed that the graphene are mainly of 1-5 layers. The magnetic field induced arc discharge method provided a low cost and eco-friendly route for the preparation of high-quality and few-layer graphene. (C) 2015 Elsevier B.V. All rights reserved.

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