4.5 Article Proceedings Paper

LSO-Based Single Crystal Film Scintillator for Synchrotron-Based Hard X-Ray Micro-Imaging

Journal

IEEE TRANSACTIONS ON NUCLEAR SCIENCE
Volume 56, Issue 3, Pages 1412-1418

Publisher

IEEE-INST ELECTRICAL ELECTRONICS ENGINEERS INC
DOI: 10.1109/TNS.2009.2015878

Keywords

LSO:Tb; luminescence; micro-imaging; micro-tomography; submicrometer resolution; synchrotron instrumentation; thin screen scintillator; X-ray detector

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X-ray detector systems are powerful tools: in combination with tomographic methods they provide volumetric data of samples in a non-destructive manner which is of high interest for, e.g., biology, medicine or materials research. The detector able to provide images with submicrometer spatial resolution frequently consists of a scintillator screen, light microscopy optics and a digital camera. Here, the scintillator converts the X-rays into a visible light image which is projected onto the camera by the light optics. In order to perform high resolution imaging Single Crystal Film (SCF) scintillators 1 mu m to 30 mu m thin are required due to the limited depth of focus of the microscopy optics. Thin SCFs can be obtained via liquid phase epitaxy (LPE). A drawback is that a detector working with SCFs suffers from low efficiency (2% at 50 keV) owing to their limited thickness. The detective quantum efficiency (DQE) is here mainly limited by the low absorption of X-rays and the light yield in the thin scintillator layer. Performances, he absorption, light yield, afterglow of operational systems at the European Synchrotron Radiation Facility (ESRF) using YAG:Ce (Y3Al5O12:Ce), LAG:Eu (Lu3Al5O12:Eu) and GGG:Eu (Gd3Ga5O12:Eu) scintillators [1] will be presented and compared to new LSO:Tb (Lu2SiO5:Tb) scintillators developed in the framework of an European project [2], [3]. A new concept to improve the efficiency of detection in the 20 keV - 40 keV energy range with 1 mu m spatial resolution will be presented. This concept based on multilayer scintillators is realised by the LPE process as well. First results will be illustrated with X-ray images and will demonstrate the absorption efficiency improvement of the X-ray detector. The expected performance is 7 times better than the LAG-based scintillators.

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