Journal
MATERIALS LETTERS
Volume 138, Issue -, Pages 116-119Publisher
ELSEVIER
DOI: 10.1016/j.matlet.2014.09.125
Keywords
Magnetic materials; Crystal growth; Phase transformation; Nanocrystalline materials
Funding
- TBU in Zlin [IGA/FT/2013/014]
- European Social Fund (ESF)
- National Budget of Czech Republic [CZ.1.07/2.3.00/20.0104, CZ.1.05/2.1.00/03.0111]
- European Regional Development Fund (ERDF)
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Iron oxide particles were prepared by a simple organic precursor assisted thermal decomposition technique. Microwaves were used as a source of energy for both precursor synthesis and generation of heat required for thermal decomposition. Ferrous oxalate dehydrate prepared within the microwave-assisted solvothermal process possess needle-like particle morphology with the length of about 20 mu m and submicrometric diameter. Magnetic iron oxide was formed by a topotactic decomposition of prepared precursor in a microwave reactor thus the final product also preserves needle-like shape and possesses soft ferrimagnetic behavior. (C) 2014 Elsevier B.V. All rights reserved
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